Study program:
Minerology and Crystallography (VII semester -MsC) |
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Name of subject: Scanning Electron Microscopy and Microanalysis |
Instructors:
Prof. Aleksandar Pačevski |
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Status: Optional |
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ECTS: 5 |
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Prerequisites: - |
Course Objectives:
Training for direct practical work on the scanning electron microscope, from sample preparation, through direct observation to the presentation of analytical data. |
Learning Outcomes:
Students are getting knowledge and skills for the independent work on the scanning electron microscope (SEM). |
Content:
Theory teaching
Basic principles of electronic microscopy - introduction; Function of important parts of the scanning electron microscope; Preparation of different types of samples and application on the supports; Basic principles of covering (gold, carbon); Attaining vacuum, entering and changing the sample, SEI and BSE images; EDS/WDS analysis; Unpolished samples - qualitative and semi-quantitative analyzes, internal standards; External standards; Polished Samples - Point and Line Quantitative Analysis; Mapping; Analytical errors; View of analytical data; Cathodoluminescence - zircon and other mineral species; Practical teaching
Practical exercises in a laboratory for scanning electron microscopy from material preparation through direct measurement to presentation and processing of results. |
Suggested Reading List:
- P.Echlin, 2009, Handbook of Sample Preparation for Scanning Electron Microscopy and X-Ray Microanalysis, 200p
- S.J.B. Reed, 2005, Electron Microprobe Analysis and Scanning Electron Microscopy in Geology
- J.I.Goldstein, at al., 2003, Scanning Elecrton Microscopy and X-Ray Microanalysis, New York, 689
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Conduct of the Course:
Lectures: Interactive with Power-Point presentations.
Exercises: Direct laboratory work on the scanning electron microscope. |
Fund hours:
| Lectures |
Exercises |
Other forms of teaching |
Study research |
| 2 |
2 |
0 |
0 |
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Assessment:
| Final Exam |
ECTS |
| Oral Exam | 30 |
| Classwork Assessment |
ECTS |
| Class Participationа | 10 | | Practical Classes | 30 | | Written tests | 30 |
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Additional Assessment Criteria: - |
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