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Instruments and Methods in Crystallography 1

Study program:
Minerology and Crystallography (VII semester -MsC)
Name of subject: Instruments and Methods in Crystallography 1
Instructors:
Prof. Aleksandar Kremenović
Status: Optional
ECTS: 5
Prerequisites: -
Course Objectives:
Different techniques for registering the intensity of diffracted X-rays on polycrystalline materials are examined. The principles of manipulation with different crystallographic instruments are studied.
Learning Outcomes:
After passing a course, students should be familiar with practical and theoretical basis in the field of X-ray analysis of polycrystalline materials.
Content:

Theory teaching
Crystal. X-rays. Bragg low. X-ray tube. Synchrotron. Neutrons. Safety procedures. Photographic techniques for X-ray detection. Electronic counters for X-ray detection. Detectors. Plotters. X-ray powder patterns registered on a film. X-ray powder diffractometry. Sample preparation.

Practical teaching
Practical exercises are closely connected to lectures. One seminar work is planed to be realized.
Suggested Reading List:
  1. Đurić, S., B., (2002) Metode istraživanja u kristalografiji, Beograd-Čačak, ITN SANU.
  2. Giacovazzo, C., Monaco, H.L., Viterbo, D., Scordari, F., Gilli, G., Zanotti, G., Catti, M., (1995) Fundamentals of Crystallography, IUCr monographs on Crystallography, Oxford University Press, Oxford.
  3. Arslanov, L.A., Fetisov, G.V., Howard, J.A.K., (1998) Crystallographic instrumentation, IUCr monographs on Crystallography, Oxford University Press, Oxford.
  4. Jenkins, R., Snyder, R.L., (1996) Introduction to X-ray powder diffraction, John Wiley and Sons, Inc., New York.
Conduct of the Course:
For the sake of active participation of students on the curse, beside classical lectures presented with aid of audio-visual methods, seminar works are planed to be realized.
Fund hours:
Lectures Exercises Other forms of teaching Study research
2 2 0 0
Assessment:
Final Exam ECTS
Written exam25
Oral Exam25

Classwork Assessment ECTS
Class Participationа20
Seminars30
Additional Assessment Criteria: -

UP!S



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